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By Edwin S. Crawley, Henry B. Evans

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1994) Introduction to Surface Chemistry and Catalysis, John Wiley & Sons, New York. C. (1997) Surface Analysis: The Principal Techniques, John Wiley & Sons, New York. W. (2008) Surface Science, 2nd edn, John Wiley & Sons, New York. A. and Li, Y. (2010) Introduction to Surface Chemistry and Catalysis, 2nd edn, John Wiley & Sons, New York. Besenbacher, F. (1996) Rep. Progr. , 59. T. (2008) Handbook of Heterogeneous Catalysis, vol. 2 (eds G. Ertl, H. Kn€ozinger, F. Sch€ uth, and J. Weitkamp), John Wiley & Sons, p.

Since the energies of core electrons are to a first approximation independent of the atomic environment, XPS is particularly useful for elemental (qualitative as well as quantitative) analysis. Typical variations of the binding energies are denoted as chemical shifts and are dependent on the bonding of the analyzed atom, in particular its oxidation state. This technique is not restricted to flat or even single crystal surfaces and is therefore frequently applied also to “real” surfaces. , up to the mbar) pressure region [35].

For the outstanding case of catalysis, the challenge is more involved because the application consists of a molecular reaction taking place at the catalyst surface. Hence characterization and reaction have to be performed in the same cell, under reaction conditions (reactants, flow, temperature, pressure, concentration, and reactor characteristics) and with simultaneous online analysis of reactants and products allowing the determination of the catalyst activity and selectivity. The cell also acts as a catalysis reactor.

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Analytic geometry by Edwin S. Crawley, Henry B. Evans


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